Gram-scale, high-yield synthesis of a robust metal–organic framework for storing methane and other gases†

Department of Chemical & Biological Eng Sheridan Road, Evanston, Illinois 60208, U Department of Chemistry and Interna Northwestern University, 2145 Sheridan E-mail: [email protected]; j-hupp@ NIST Center for Neutron Research, Nationa Gaithersburg, MD 20899, USA. E-mail: tane Department of Materials Science and E Philadelphia, PA 19104, USA † Electronic supplementary information materials, and instrumentations; synthe NMR) of LH6; synthesis and X-ray crystal sorption isotherms, BET analysis a 10.1039/c3ee24506c ‡ These authors contributed equally. § C.E.W. and O.K.F. designed the researc guidance from R.Q.S. O.K.F. and I.E. syn and activated NU-125. A.A.S. solved t performed the high-pressure measur interpretation and contributed to MOF-activation methodology. All authors on the manuscript. The manuscript was authors. All authors have given approval t Cite this: Energy Environ. Sci., 2013, 6, 1158